HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 12246538, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Peracetic Acid | HCID 6585 | — |
| Reactant | HCID 238592 | HCID 238592 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 12246538 | HCID 12246538 | — |
Reaction Steps
To a mixture of phenyl-2-thienyl ketone hydrazone (20.2 g; 0.1 mole), and pyridine (24.8 ml; 0.307 mole) in N,N-dimethylacetamide (100 ml) stirred and cooled to 15° was added peracetic acid (17.7 ml of a 38% w/w solution in glacial acetic acid; 0.1 mole) during 40 minutes, the temperature being maintained at +15° throughout.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04083837 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-e06efc0682284a90832d45e4d164069e |
| Source note | uspto-grants-1978_04 |