HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 20359121, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 20359072 | HCID 20359072 | — |
| Reactant | HCID 22760509 | HCID 22760509 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 20359121 | HCID 20359121 | — |
Reaction Steps
3.7 g (0.01 mol) of 3'-acetylsulfamoyl-2-bromo-4'-chloroacetophenone are stirred at 20° C during 24 hours in 20 ml of ethyl acetate with 1.8 g (1.01 mol) of 1-ethyl-3-(2-methoxypropyl)thiourea, 60 ml of ether are added and the amorphous oily precipitate is solidified by trituration after under 40 ml of ether decanting the solvent. Amorphous solid substance capable of flowing, decomposition starting at 65° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04083979 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-416720ec627f41948ec9ef9a872d5a22 |
| Source note | uspto-grants-1978_04 |