HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 123606999, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Diethyl chlorophosphate | HCID 13139 | — |
| Reactant | HCID 123697742 | HCID 123697742 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 123606999 | HCID 123606999 | — |
Reaction Steps
The reaction described in Example 10 was carried out using 2-(diphenylmethylsilyl)-ethanol (2.25 g), diethylphosphorochloridate (1.35 g), and pyridine (0.6 g) in carbon tetrachloride (10 ml). Diethyl 2-(diphenylmethylsilyl)ethyl phosphate was obtained as a colourless oil (1.35 g) (C17H23Si O4P requires: C, 60.5%; H, 7.1%; Found: C 63.4%; H, 7.8%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04084951 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-35b8946bef7f4be4a5335c9e5f165e17 |
| Source note | uspto-grants-1978_04 |