反应详情

In a manner similar to that of Example 2 (A), 4.80 g (33.5 mmol) of 1,4,7-triazacyclodecane and 4.00 g of dimethylformamide dimethyl acetal were reacted to give 4.67 g (91%) of clear, colorless liquid, bp 96°-97.5° (4.0 mm). Redistillation in a molecular still at 70° (3.4 mm) gave an analytical sample of 1,4,7-triazatricyclo[5.3.1.04,11 ]-undecane.

1. customto give 4.67 g (91%) of clear, colorless liquid, bp 96°-97.5° (4.0 mm)
2. distillationRedistillation in a molecular still at 70° (3.4 mm)