Hydrogen Bromide → HCID 21332377, compound

HRID 2083348Notes

Reaction equation

Br.[CH2:2]([N:17]([CH2:19][CH:20]([OH:29])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28])C)[CH2:3][N:4]([CH2:6][CH:7]([OH:16])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])C>>[CH2:3]([NH:4][CH2:6][CH:7]([OH:16])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])[CH2:2][NH:17][CH2:19][CH:20]([OH:29])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28]

Participants

Reactant 2

HCID 260Hydrogen Bromide

HCID 21332424HCID 21332424, compound

Product 1

HCID 21332377HCID 21332377, compound

Procedure

In a manner similar to that of Example 22, methylation of N,N'-ethylenebis[2-hydroxydecylamine] (15 g.) and treatment of the resulting product with hydrogen bromide gave N,N'-ethylenebis[N-methyl-2-hydroxydecylamine] (I: R = CH3 (CH2)7, R' = CH3, X = (CH2)2, Z = H) dihydrobromide (4.0 g., m.p. 152.0°-164.0° C.).

Sources & evidence

ORD record: ord-b802ff40ab214ad4ab0725f5b34ed1fd
Source dataset: uspto-grants-1978_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04085144

Reaction notes

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