Methyl Isocyanate → HCID 20394652, compound

HRID 2083559Notes

Reaction equation

HRID 2083559 reaction equation
[C:1]([C:5]1[S:6][C:7]([NH:10][CH2:11][CH3:12])=[N:8][N:9]=1)([CH3:4])([CH3:3])[CH3:2].[CH3:13][N:14]=[C:15]=[O:16]>O>[CH2:11]([N:10]([C:7]1[S:6][C:5]([C:1]([CH3:4])([CH3:2])[CH3:3])=[N:9][N:8]=1)[C:15]([NH:14][CH3:13])=[O:16])[CH3:12]

Participants

4

Reactant 2

HCID 12228Methyl IsocyanateHCID 20356529HCID 20356529, compound

Product 1

HCID 20394652HCID 20394652, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of 9.25 g of 2-tert.butyl-5-ethylamino-1,3,4-thiadiazole and 3.5 g of methyl isocyanate is heated several hours on the steam bath and poured into water to give 1-ethyl-1-(5-tert.butyl-1,3,4-thiadiazol-2-yl)-3-methylurea, m.p. 112°.

Sources & evidence

ORD record
ord-2e1f7a2ec8cb475b82839906435a0724
Source dataset
uspto-grants-1978_04
Patent number
US04086077

Reaction notes

Loading…