HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 20394652, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | 5-tert-butyl-N-ethyl-1,3,4-thiadiazol-2-amine | HCID 20356529 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20394652 | HCID 20394652 | — |
Reaction Steps
A solution of 9.25 g of 2-tert.butyl-5-ethylamino-1,3,4-thiadiazole and 3.5 g of methyl isocyanate is heated several hours on the steam bath and poured into water to give 1-ethyl-1-(5-tert.butyl-1,3,4-thiadiazol-2-yl)-3-methylurea, m.p. 112°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04086077 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-2e1f7a2ec8cb475b82839906435a0724 |
| Source note | uspto-grants-1978_04 |