Hydrochloric Acid → HCID 20300399, compound

Participants

Reaction Steps

A solution of 158 g. of 1-chloro-2-nitrobenzene and 260 g. of 1-ethyl propylamine are refluxed together for 5 days. The solution is cooled and 500 ml. of water is added followed by 10 ml. of concentrated hydrochloric acid. The product separates out as an oil and is extracted with chloroform (2 × 200 ml.). The chloroform layer is dried over MgSO4 and evaporated to yield 190 g. (91%) of product.

Provenance & Evidence