HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 20356980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 4-Bromo-2,2-diphenylbutyronitrile | HCID 96575 | — |
| Reactant | 5-chloro-2,2-diphenylpentanenitrile | HCID 324019 | — |
| Reactant | (+-)-1,4-Diazabicyclo[4.4.0]decane | HCID 2876391 | — |
| Product | HCID 20356980 | HCID 20356980 | — |
Reaction Steps
Substitution of an equivalent quantity of 2,2-diphenyl-5-chlorovaleronitrile for the 2,2-diphenyl-4-bromobutyronitrile, and 1,4-diazabicyclo[4.4.0]decane for the piperidine used in Example 22, and substantial repetition of the procedure detailed therein, affords 2,2-diphenyl-5-(1,4-diazabicyclo[4.4.0]dec-4-yl)valeronitrile dihydrochloride, melting at about 233° - 238° C. with decomposition.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04086234 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-f5451d53b0244d27bb5d4f2098e4ea01 |
| Source note | uspto-grants-1978_04 |