HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 20357868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | methyl N-(p-nitrobenzyloxycarbonyl)-alpha-methoxyglycinate | HCID 20357887 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20357868 | HCID 20357868 | — |
Reaction Steps
Aqueous sodium hydroxide (10 ml of a 2.5 N solution) is added dropwise over 15 minutes to a stirring solution of methyl N-(p-nitrobenzyloxycarbonyl)-α-methoxyglycinate (7.46 g, 25 mMol) in methanol (5 ml). The methanol is removed under reduced pressure and the aqueous residue is lyophilized to give sodium N-(p-nitrobenzyloxycarbonyl)-α-methoxyglycinate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04086423 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-3ce6ec277ffa44f997e91fda260ba89e |
| Source note | uspto-grants-1978_04 |