HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178446044, compound → HCID 178446031, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178446044 | HCID 178446044 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178446031 | HCID 178446031 | — |
Reaction Steps
A solution of 6.43 g. of Nα -benzyloxycarbonyl-L-leucyl-L-arginyl-L-prolyl-glycinamide hydrochloride in 200 ml. of methanol with 250 mg. of 20% palladium-on-carbon is stirred under hydrogen gas for three hours, the catalyst removed by filtration, and the filtrate evaporated to dryness at 45° C. under reduced pressure. The dried residue is a foam which is suitable for use without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04086219 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-9be47c47ea9d4073a0a99af9c98ec86c |
| Source note | uspto-grants-1978_04 |