HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2083922Generated: October 31, 2026
2,4-Dichlorophenethylamine → HCID 86586630, compound
https://huagongshe.com/reaction/2083922
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2,4-Dichlorophenethylamine | HCID 142938 | — |
| Reactant | 4-Nitrophthalic acid anhydride | HCID 230976 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86586630 | HCID 86586630 | — |
Reaction Steps
2-(2,4-dichlorophenyl)ethanamine was suspended in toluene with 4-nitrophthalic anhydride (1 eq) and heated to 150° C. After 2 hours, the reaction was cooled and checked for completion by LC/MS. The solvent was then removed in vacuo and the resulting product was taken on to the next step without further purification. Rt 3.91 minutes, LC/MS m/z 365.1 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06716840B2 |
|---|
| Source dataset | uspto-grants-2004_04 |
|---|
| ORD ID | ord-f043fec795a440149cefdc30dd8b7835 |
|---|
| Source note | uspto-grants-2004_04 |
|---|
