Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 12531835 | HCID 12531835 | — |
| Solvent | Dimethyl Carbonate | HCID 12021 | — |
| Product | HCID 69782740 | HCID 69782740 | — |
Reaction Steps
A suspension of sodium hydride (350 mg) in dimethyl carbonate (10 ml) is treated at room temperature with the product obtained in step D. The mixture is heated to 90° C. for 1 hour, cooled and poured into ice water and extracted with methylene chloride. The extract is dried and evaporated to yield 5.7 of the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06716845B2 |
|---|
| Source dataset | uspto-grants-2004_04 |
|---|
| ORD ID | ord-02c63340c41a44f0976d26e93c163e14 |
|---|
| Source note | uspto-grants-2004_04 |
|---|
