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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2083999Generated: November 4, 2026

HCID 22732612, compound → HCID 22732610, compound

https://huagongshe.com/reaction/2083999

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22732612HCID 22732612—
CatalystPalladiumHCID 23938—
SolventDimethylformamideHCID 6228—
ProductHCID 22732610HCID 22732610—

Reaction Steps

1 g (2.3 mmol) of 5-(4′-nitrobiphenyl-4-sulfonyl)-1-methyl-4,5,6,7-tetrahydro-1H-imidazo[4,5-c]pyridine-6-carboxylic acid was dissolved in 15 ml of dimethylformamide (DMF) and, after addition of 0.1 g of hydrogenation catalyst (10% Pd on activated carbon), quantitatively hydrogenated within 2 h. After removal of the solvent, the crude product was purified by chromatography.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06716853B2
Source datasetuspto-grants-2004_04
ORD IDord-e1852b5133f74e88b536aa1af414a1ad
Source noteuspto-grants-2004_04