HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22732612, compound → HCID 22732610, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22732612 | HCID 22732612 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22732610 | HCID 22732610 | — |
Reaction Steps
1 g (2.3 mmol) of 5-(4′-nitrobiphenyl-4-sulfonyl)-1-methyl-4,5,6,7-tetrahydro-1H-imidazo[4,5-c]pyridine-6-carboxylic acid was dissolved in 15 ml of dimethylformamide (DMF) and, after addition of 0.1 g of hydrogenation catalyst (10% Pd on activated carbon), quantitatively hydrogenated within 2 h. After removal of the solvent, the crude product was purified by chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716853B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-e1852b5133f74e88b536aa1af414a1ad |
| Source note | uspto-grants-2004_04 |