HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl iodide → HCID 10199064, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl iodide | HCID 6362 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 10036272 | HCID 10036272 | — |
| Solvent | Toluene | HCID 1140 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 10199064 | HCID 10199064 | — |
Reaction Steps
Prepared from 6-(2-(Diethylamino)ethyl)-indole (14 mg, 0.0647 mmol), 2-iodopropane (44 μl, 0.259 mmol), NaH (3.1 mg, 0.129 mmol), K2CO3 (35 mg, 0.259 mmol) in 0.1 ml of DMF and 0.5 ml of toluene, according to example. Yield 8.5 mg (51%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716837B1 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-8c8d706cecf44a9a80d94e2ad160031c |
| Source note | uspto-grants-2004_04 |