HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylcarbamoyl Chloride → HCID 9903906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylcarbamoyl Chloride | HCID 6598 | — |
| Reactant | Sodium bis(trimethylsilyl)amide | HCID 2724254 | — |
| Reactant | 6-(1-Methyl-1,2,3,6-tetrahydropyridin-4-yl)-1H-indole | HCID 10130559 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 9903906 | HCID 9903906 | — |
Reaction Steps
From 6-(1-Methyl-1,2,5,6-tetrahydropyridin-4-yl)-indole (16.6 mg, 0.0735 mmol), dimethylcarbamyl chloride (15.8 mg. 0.147 mmol) and 1M NaN(TMS)2(0.147ml) in 0.5 ml of THF at 0° C. Yield 12.5 mg (60%), the reaction being carried out according to Example 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716837B1 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-a802f2fc95d04ee796d6ed0c52d798c1 |
| Source note | uspto-grants-2004_04 |