HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Methylhydroxylamine hydrochloride → HCID 85340123, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Methylhydroxylamine hydrochloride | HCID 521874 | — |
| Reactant | HCID 22733081 | HCID 22733081 | — |
| Product | HCID 85340123 | HCID 85340123 | 70% |
Reaction Steps
0.3 g (1.47 mmol) of 1-(2-oxo-2-pyridin-3-yl-ethyl)-pyrrolidin-2-one prepared from Example 20 and 0.18 g (2.21 mmol) of methoxyamine hydrochloride salt were treated as described in Example 22 to obtain 0.24 g (70% yield) of 1-(2-methoxyimino-2-pyridin-3-yl-ethyl)-pyrrolidin-2-one as E/Z mixture (2.38:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716857B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-5fd7cffd7cc54eaab6716a8e29cf0af1 |
| Source note | uspto-grants-2004_04 |