HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoyl chloride → HCID 9802268, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | N1-[1-(4-pyridyl)piperidin-4-ylmethyl)-1,2-benzenediamine | HCID 12150698 | — |
| Product | HCID 9802268 | HCID 9802268 | 55.2% |
Reaction Steps
Using a similar procedure to that described in Example 2, Part D, N1-[1-(4-pyridyl)piperidin-4-ylmethyl)-1,2-benzenediamine (167 mg, 0.59 mmol) and 4-chlorobenzoyl chloride (0.075 mL, 0.59 mmol) yielded 137 mg (55%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716855B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-ea8499bb66a7425b9cce65558071a0f4 |
| Source note | uspto-grants-2004_04 |