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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2084362Generated: October 31, 2026

HCID 69830277, compound → HCID 12109867, compound

https://huagongshe.com/reaction/2084362

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69830277HCID 69830277—
ReactantHCID 178418361HCID 178418361—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductHCID 12109867HCID 1210986797.9%

Reaction Steps

To a solution of (2R)-1-(benzyloxy)-3-(1H-imidazol-2-yl)-2-propanol (424 mg) in methanol (10 ml), 10% palladium carbon (50% hydrated, 85 mg) was added, followed by stirring at 50-60° C. in a hydrogen atmosphere for 2 days. The catalyst was filtered off; the filtrate was concentrated to yield the titled compound (254 mg) as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06716863B2
Source datasetuspto-grants-2004_04
ORD IDord-16c911c5cf564035b6fb0b14d201fd51
Source noteuspto-grants-2004_04