HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → 3-(3-Benzyloxyphenyl)propyl methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 3-(Phenylmethoxy)benzenepropanol | HCID 12648155 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 3-(3-Benzyloxyphenyl)propyl methanesulfonate | HCID 22733363 | — |
Reaction Steps
Using 3-(3-benzyloxyphenyl)propanol (13.5 g), triethylamine (8.16 ml) and methanesulfonyl chloride(4.53 ml), the same reaction as Reference Example 9-(iv) was carried out to yield the titled compound (19.7 g) as an oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716863B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-ea30888403ac49ffa83dfa8aa20e4d0f |
| Source note | uspto-grants-2004_04 |