HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → Benzyl 3-(3-iodopropyl)phenyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | 3-(3-Benzyloxyphenyl)propyl methanesulfonate | HCID 22733363 | — |
| Product | Benzyl 3-(3-iodopropyl)phenyl ether | HCID 22733348 | 85% |
Reaction Steps
Using 3-[3-(benzyloxy)phenyl]propyl methanesulfonate (19.7 g) and sodium iodide (29.25 g), the same reaction as Reference Example 9-(v) was carried out to yield the titled compound (18.4 g) as an oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716863B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-4ff323bc330e495cb51fb2088897581a |
| Source note | uspto-grants-2004_04 |