HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-Hydroxybutyl)phenol → HCID 22733356, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-Hydroxybutyl)phenol | HCID 13392513 | — |
| Reactant | HCID 22259301 | HCID 22259301 | — |
| Product | HCID 22733356 | HCID 22733356 | 91% |
Reaction Steps
Using 4-(4-hydroxyphenyl)-1-butanol (4.99 g) and (E)-4-chloromethyl-2-[2-(4-bromophenyl)ethenyl]oxazole (7.43 g), the same reaction as Reference Example 17-(i) was carried out to yield 4-[4-[2-(E)-[2-(4-bromophenyl)ethenyl]-1,3-oxazol-4-yl]methoxyphenyl]-1-butanol (9.70 g). Using the compound obtained (4.28 g), the same reaction as Reference Example 17-(ii) was carried out to yield the titled compound (4.47 g) as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716863B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-4e650969743249589a407e08a19f84a3 |
| Source note | uspto-grants-2004_04 |