HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 136388368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 60077773 | HCID 60077773 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 136388368 | HCID 136388368 | — |
Reaction Steps
(1(S)-tert-Butyl-2-oxo-3-pyridin-2-yl-propyl)-carbamic acid tert-butyl ester (300 mg, 1.0 mmol), was dissolved in dioxane saturated with HCl (20 mL) and the reaction mixture stirred at room temperature for 2 hours. The mixture was then concentrated in vacuo to give the title compound as a yellow solid (0.37 g) which was used in Step C without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716878B1 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-9800897a7b3f4d61b03359d8b0e491c9 |
| Source note | uspto-grants-2004_04 |