HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 22733447, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | 4-Aminobenzene-1,3-diol hydrochloride | HCID 13408822 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22733447 | HCID 22733447 | — |
Reaction Steps
A mixture of 1.01 ml of pivaloyl chloride, 808 mg 2,4-dihydroxyaniline hydrochloride (formula V) and 0.4 ml of pyridine is heated at about 210° for about 18 hours. The mixture obtained is dispersed in a mixture of cyclohexane and ethyl acetate and purified by chromatography. The title compound is obtained (m.p. 204-210°).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716865B1 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-7732a6878de642618b62e9ac97ff4b2c |
| Source note | uspto-grants-2004_04 |