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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2084685Generated: October 31, 2026

Diethyl Ether → HCID 22734530, compound

https://huagongshe.com/reaction/2084685

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl EtherHCID 3283—
ReactantDimethylformamideHCID 6228—
Reactant1-[(4-methylphenyl)sulfonyl]-1H-indol-4-olHCID 10379309—
SolventAllyl bromideHCID 7841—
SolventPotassium CarbonateHCID 11430—
ProductHCID 22734530HCID 22734530—

Reaction Steps

Treatment of 1-[(4-methylphenyl)sulfonyl]-1H-indol-4-ol with potassium carbonate and allyl bromide in N,N-dimethylformamide (29.24 g, 0.242 mol) followed by aqueous workup and extraction with diethyl ether provides 4-(allyloxy)-1-[(4-methylphenyl)sulfonyl]-1H-indole.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06716998B2
Source datasetuspto-grants-2004_04
ORD IDord-4ecce77003b84c6cb1ba26f32e449466
Source noteuspto-grants-2004_04