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HRID2084685

反应详情

EQUATION

反应方程式

HRID 2084685 的结构方程式

REACTANTS

反应物

3
结构：CCOCC
HCID3283

Diethyl Ether

C4H10O

结构：CN(C)C=O
HCID6228

N,N-Dimethylformamide

C3H7NO

结构：Cc1ccc(S(=O)(=O)n2ccc3c(O)cccc32)cc1
HCID10379309

1-[(4-methylphenyl)sulfonyl]-1H-indol-4-ol

C15H13NO3S

PRODUCTS

生成物

1
结构：C=CCOc1cccc2c1ccn2S(=O)(=O)c1ccc(C)cc1
HCID22734530

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：C=CCBr
溶剂HCID7841

Allyl bromide

C3H5Br

结构：O=C([O-])[O-].[K+].[K+]
溶剂HCID11430

Potassium Carbonate

CK2O3

PROCEDURE

实验过程

Treatment of 1-[(4-methylphenyl)sulfonyl]-1H-indol-4-ol with potassium carbonate and allyl bromide in N,N-dimethylformamide (29.24 g, 0.242 mol) followed by aqueous workup and extraction with diethyl ether provides 4-(allyloxy)-1-[(4-methylphenyl)sulfonyl]-1H-indole.