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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2084998Generated: November 2, 2026

HCID 22728659, compound → HCID 22728640, compound

https://huagongshe.com/reaction/2084998

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22728659HCID 22728659—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 22728640HCID 22728640—

Reaction Steps

A mixture of 3-[(4-nitrophenyl)thio]benzoic acid (11.2 g, 40.7 mmol) and 10% Pd/C (0.5 g) in ethanol (250 mL) was hydrogenated at atmospheric temperature and pressure for 24 h. The mixture was filtered through Celite and concentrated in vacuo to give the required aniline as a solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06719520B2
Source datasetuspto-grants-2004_04
ORD IDord-5a8a838edbbd4fae980a0442c3976003
Source noteuspto-grants-2004_04