HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22728659, compound → HCID 22728640, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22728659 | HCID 22728659 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22728640 | HCID 22728640 | — |
Reaction Steps
A mixture of 3-[(4-nitrophenyl)thio]benzoic acid (11.2 g, 40.7 mmol) and 10% Pd/C (0.5 g) in ethanol (250 mL) was hydrogenated at atmospheric temperature and pressure for 24 h. The mixture was filtered through Celite and concentrated in vacuo to give the required aniline as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06719520B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-5a8a838edbbd4fae980a0442c3976003 |
| Source note | uspto-grants-2004_04 |