Potassium Carbonate → HCID 60078031, compound

HRID 2085193Notes

Reaction equation

HRID 2085193 reaction equation
[CH3:1][N:2]([CH3:17])[S:3]([C:6]1[O:10][C:9]2[CH:11]=[CH:12][CH:13]=[C:14]([O:15][CH3:16])[C:8]=2[CH:7]=1)(=[O:5])=[O:4].S(C1C=CC([N+]([O-])=O)=CC=1)(OC[C@H:23]1[O:25][CH2:24]1)(=O)=O.C(=O)([O-])[O-].[K+].[K+]>>[CH3:1][N:2]([CH3:17])[S:3]([C:6]1[O:10][C:9]2[CH:11]=[CH:12][CH:13]=[C:14]([O:15][CH2:16][C@H:24]3[O:25][CH2:23]3)[C:8]=2[CH:7]=1)(=[O:5])=[O:4]

Participants

4

Reactant 3

HCID 11430Potassium CarbonateHCID 10868995(S)-(+)-Glycidyl-4-nitrobenzoateHCID 22729140HCID 22729140, compound

Product 1

HCID 60078031HCID 60078031, compound

Procedure

By the reactions in the same manner as in Starting Material Synthesis Example 1 using 2-(N,N-dimethylsulfamoyl)-4-methoxybenzo(b)furan (1.10 g), (S)-glycidyl nosylate (1.30 g) and potassium carbonate (1.89 g), a crude product of the title compound was quantitatively obtained as a pale-yellow oil.

Sources & evidence

ORD record
ord-2223c1400487415293728ff334e575b7
Source dataset
uspto-grants-2004_04
Patent number
US06720320B2

Reaction notes

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