Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 5(4H)-Oxazolone, 4-[(2-methoxyphenyl)methylene]-2-methyl- | HCID 361416 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68790005 | HCID 68790005 | — |
Reaction Steps
4-(2′-Methoxybenzylidene)-2-methyl-4H-oxazol-5-one (5 g) was dissolved in ethanol (100 ml) and aqueous methylamine solution (20 ml) and potassium carbonate (7 g) were added. The mixture was heated at 80° C. for 7 hr. After cooling, the solvent was evaporated under reduced pressure and the precipitated yellow crystals were collected by filtration to give the title compound (2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06720320B2 |
|---|
| Source dataset | uspto-grants-2004_04 |
|---|
| ORD ID | ord-8b0de6a036e443d3a5093007010d941d |
|---|
| Source note | uspto-grants-2004_04 |
|---|
