HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 22282584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22282647 | HCID 22282647 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22282584 | HCID 22282584 | 99% |
Reaction Steps
Thionyl chloride (2 mL) was added to a suspension of 4-(2H-chromen-4-yl)benzoic acid from reaction 34c (0.415 g, 1.6 mmol) in dichloromethane (10 mL) at room temperature. The reaction was stirred for 4 h, concentrated in vacuo to give 4-(2H-chromen-4-yl)benzoyl chloride (0.445 g, 99%) as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06720329B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-898ad14979704cb48529cba8deeebee5 |
| Source note | uspto-grants-2004_04 |