Pentane → HCID 22731334, compound

Participants

Reaction Steps

Following General Procedure A and using 5-bromo-7-cyclohexylmethyl-3,3-dimethyl-2,3-dihydro-benzofuran (Intermediate 46, 0.58 g, 1.79 mmol),15 mL of anhydrous diethyl ether, 1.7M solution of t-butyllithium in n-pentane (2.21 mL, 3.77 mmol) and trimethyl borate (0.42 mL, 3.77 mmol) the title compound was obtained as a foam that was used as such for the next step without purification and characterization.

Provenance & Evidence