Trifluoroacetic acid → HCID 69827417, compound

Participants

Reaction Steps

To a solution of [2-[4-chloro-3-(tricyclo[3.3.1.13,7]dec-1-ylmethyl)carbamoyl-phenylamino]-ethylamino]-propionic acid, 1,1-dimethylethyl ester (0.20 g, Example 7a) in dichloromethane (5 ml), was added trifluoroacetic acid (2 ml). After 15 h the solution was concentrated and purified by RPHPLC (eluting with 15-95% MeCN in 0.1% AcONH4 aqueous) to afford the title compound as a solid (0.010 g).

Provenance & Evidence