HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 22730840, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 22730792 | HCID 22730792 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22730840 | HCID 22730840 | — |
Reaction Steps
A solution of Example 201H (1.65 g, 4.92 mmol) in dichloromethane (15 mL) at room temperature was treated oxalyl chloride (344 mg, 2.71 mmol), stirred for 20 minutes, treated with toluene (25 mL), and concentrated to provide the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06720338B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-a67bd1e8aea2444295db5e473a9d4fcf |
| Source note | uspto-grants-2004_04 |