反应详情

To a stirred solution of 1-(2-t-butyloxycarbonylaminoethylthio)-3-chloropropan-2-one (11.47 g, 42.8 mmol) in methanol (50 mL) was added ammonium dithiocarbamate (4.73 g, 42.9 mmol) at room temperature. After 50 hours the reaction mixture was partitioned between ethyl acetate and water.

1. customAfter 50 hours the reaction mixture was partitioned between ethyl acetate and water