HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium dithiocarbamate → HCID 178453854, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium dithiocarbamate | HCID 11083854 | — |
| Reactant | 1-(2-t-Butyloxycarbonylaminoethylthio)-3-chloropropan-2-one | HCID 22726740 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178453854 | HCID 178453854 | — |
Reaction Steps
To a stirred solution of 1-(2-t-butyloxycarbonylaminoethylthio)-3-chloropropan-2-one (11.47 g, 42.8 mmol) in methanol (50 mL) was added ammonium dithiocarbamate (4.73 g, 42.9 mmol) at room temperature. After 50 hours the reaction mixture was partitioned between ethyl acetate and water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06723716B1 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-1fbf8a2731724f7299b56df31e0ad0d0 |
| Source note | uspto-grants-2004_04 |