Zincchloride → Sodium Chloride

HRID 2086077Notes

Reaction equation

HRID 2086077 reaction equation
[Cl-:1].[Zn+2:2].[Cl-].[C:4]([BH3-:6])#[N:5].[Na+:7]>CO>[C:4]([BH3-:6])#[N:5].[Zn+2:2].[C:4]([BH3-:6])#[N:5].[Cl-:1].[Na+:7]

Participants

5

Reactant 2

HCID 3007855ZincchlorideHCID 5003444Sodium cyanoborohydride

Product 2

HCID 5234Sodium ChlorideHCID 131724416HCID 131724416, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

Anhydrous zinc chloride (15.4 g, 0.11 mol) was dissolved in methanol (250 ml) and then treated with sodium cyanoborohydride (14.2 g, 0.23 mmol). After stirring for 15 minutes at ambient temperature a further quantity of methanol (200 ml) was added giving a colourless solution of zinc cyanoborohydride together with a small quantity of solid sodium chloride.

Workup

  1. additionwas added

Sources & evidence

ORD record
ord-a1ab6a20d16e440ea5ddc48ab7dc5778
Source dataset
uspto-grants-2004_04
Patent number
US06723735B1

Reaction notes

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