HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-dibenzyl-piperidine-4-carboxylic acid ethyl ester → HCID 22225015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-dibenzyl-piperidine-4-carboxylic acid ethyl ester | HCID 10497176 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22225015 | HCID 22225015 | 81% |
Reaction Steps
Was prepared from 1,4-dibenzyl-piperidine-4-carboxylic acid ethyl ester (J. Chem. Soc., Perkin Trans. 1 1996, 20, 2545-2551.) by lithium aluminium hydride reduction in tetrahydrofurane under standard conditions in 81% yield. MS 296(M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06727247B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-ca754187376f4f79a4b6e5d116801871 |
| Source note | uspto-grants-2004_04 |