HCID 22725080, compound → HCID 22725104, compound

Participants

Reaction Steps

Follow the procedure of Step 6 of Example 15, using the product from Step 5 (69 mg) and Lindlar catalyst (7 mg) to produce the title compound. 1H NMR (CDCl3) 8.40 (d, 1H), 7.95 (d, 2H), 775 (d, 1H), 7.05-7.15 (m, 7H), 5.60 (s, 1H), 5.25 (b, s, 1H), 4.40 (s, 2H), 3.20 (s, br, 2H), 2.50 (dd, 2H), 2.3 (m, 4H), 1.75 (d, 2H).

Provenance & Evidence