Hydrochloric Acid → HCID 22725089, compound

Participants

Reaction Conditions

Reaction Steps

Add HCl (1N in ether, 0.36 ml) to a solution of the product from Step 2 (11 mg, 0.018 mmol) in CH2Cl2 at RT for 24 h. Add HCl (1N in ether, 0.36 ml) and stir at RT for 24 h. Add another 0.36 ml of HCl (1N in ether ) and stir at 30° C. for 24 h. Concentrate, treat with ether and filter to give the title compound as white solid. ESI-MS 497.1 (100, M+).

Provenance & Evidence