HCID 22218541, compound → HCID 22723933, compound

Participants

Reaction Steps

A mixture of 542.9 mg (2.0 mmol) of 12-(4-morpholinyl)-1-dodecanol and 3.0 g of (5.10 mmol) of bis(trimethylsilyl)chromate (M. Heravi, Monatsh. Chem. 1998, 129(12), 1305-1308) in 10 ml of dichloromethane is stirred at room temperature overnight and filtered. After removal of the dichloromethane, the residue is purified by silica gel column chromatography to give 210 mg (39%) of 12-(4-morpholinyl)-1-dodecanal.

Provenance & Evidence