HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 22726020, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 4,5,6,7-Tetrahydro-N6-propyl-2,6-benzothiazolediamine | HCID 4885 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22726020 | HCID 22726020 | — |
Reaction Steps
4.00 g of (±)-2-amino-6-propylamino-4,5,6,7-tetrahydrobenzothiazole was dissolved in 10 mL of hot methanol and 2.2 mL of 48% hydrobromic acid was added. The obtained suspension was stirred, cooled and precipitated solid was filtered off. The cake was washed with cold methanol and air-dried to give 2.7 g of (±)-2-amino-6-propylamino-4,5,6,7-tetrahydrobenzothiazole monohydrobromide with m.p. 236-245° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06727367B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-48c73cce3c344b4faecc611f4e487d12 |
| Source note | uspto-grants-2004_04 |