HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,5,6,7-Tetrahydro-N6-propyl-2,6-benzothiazolediamine → HCID 22726019, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,5,6,7-Tetrahydro-N6-propyl-2,6-benzothiazolediamine | HCID 4885 | — |
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 22726019 | HCID 22726019 | — |
Reaction Steps
11.0 g of (±) 2-amino-6-propylamino-4,5,6,7-tetrahydrobenzothiazole was dissolved in 180 mL of hot isopropanol and 3.8 mL of methanesulfonic acid was added. The formed precipitate was filtered off after cooling and dried to give 10.2 g of crystals with m.p. 227-237° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06727367B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-4657c2dbe2d447818139b17591215d95 |
| Source note | uspto-grants-2004_04 |