HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(3,5-Dichlorophenoxy)furan-2-carbonyl chloride → 5-(3,5-Dichlorophenoxy)-N-(4-{4-[3-(isobutyrylamino)phenyl]-1-piperidinyl}butyl)-2-furamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(3,5-Dichlorophenoxy)furan-2-carbonyl chloride | HCID 2736028 | — |
| Reactant | N-{3-[1-(4-Aminobutyl)4-piperidinyl]phenyl}-2-methylpropanamide | HCID 16757471 | — |
| Solvent | Tetrahydrofurane dichloromethane | HCID 21919333 | — |
| Product | 5-(3,5-Dichlorophenoxy)-N-(4-{4-[3-(isobutyrylamino)phenyl]-1-piperidinyl}butyl)-2-furamide | HCID 22049530 | — |
Reaction Steps
Prepared by Procedure Q2 (THF/DCM, 1:3) and Scheme AT using N-{3-[1-(4-aminobutyl)-4-piperidinyl]phenyl}-2-methylpropanamide and 5-(3,5-dichlorophenoxy)-2-furoyl chloride: ESMS m/e: 572.0 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06727264B1 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-d0feceae64b44a0e89a4b4dff275733e |
| Source note | uspto-grants-2004_04 |