Potassium Carbonate → HCID 22049066, compound

HRID 2087828Notes

Reaction equation

HRID 2087828 reaction equation
C([O-])([O-])=O.[K+].[K+].[I:7][C:8]1[CH:9]=[C:10]([C:14](=[O:20])[CH2:15][CH2:16][CH2:17][CH2:18]Cl)[CH:11]=[CH:12][CH:13]=1.[CH3:21][CH:22]([CH3:38])[C:23]([NH:25][C:26]1[CH:31]=[CH:30][CH:29]=[C:28]([CH:32]2[CH2:37][CH2:36][NH:35][CH2:34][CH2:33]2)[CH:27]=1)=[O:24]>>[I:7][C:8]1[CH:9]=[C:10]([C:14](=[O:20])[CH2:15][CH2:16][CH2:17][CH2:18][N:35]2[CH2:36][CH2:37][CH:32]([C:28]3[CH:27]=[C:26]([NH:25][C:23](=[O:24])[CH:22]([CH3:21])[CH3:38])[CH:31]=[CH:30][CH:29]=3)[CH2:33][CH2:34]2)[CH:11]=[CH:12][CH:13]=1

Participants

4

Reactant 3

HCID 11430Potassium CarbonateHCID 167572552-methyl-N-[3-(4-piperidyl)phenyl]propanamideHCID 220489265-Chloro-1-(3-iodophenyl)pentan-1-one

Product 1

HCID 22049066HCID 22049066, compound

Procedure

Prepared by Procedure K and Scheme B1 (K2CO3) using 1-(3-iodophenyl)-5-chloro-1-pentanone and 2-methyl-N-[3-(4-piperidinyl)phenyl]propanamide: ESMS m/e: 533.0 (M+H)+.

Sources & evidence

ORD record
ord-d1da9d2242fd4e798249fb76c82d41d2
Source dataset
uspto-grants-2004_04
Patent number
US06727264B1

Reaction notes

Loading…