HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(trifluoromethyl)pyridine-2-carboxylic Acid → HCID 59331162, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(trifluoromethyl)pyridine-2-carboxylic Acid | HCID 10910349 | — |
| Reactant | HCID 44286533 | HCID 44286533 | — |
| Product | HCID 59331162 | HCID 59331162 | — |
Reaction Steps
Title compound was synthesized according to the procedure used in the synthesis of Compound 19S, using 5-(trifluoromethyl)picolinic acid in place of o-methoxybenzoic acid. 1H NMR (400 MHz, CDCl3) δ (ppm): 8.98 (s, 1H), 8.22 (dd, J=8 Hz, 1H), 7.71 (d, J=8 Hz, 1H), 6.36 (s, 1H), 4.11 (m, 1H), 3.39 (dd, J=16 Hz, 1H), 2.83-2.77 (m, 4H), 2.56 (ddd, J=16 Hz, 1H), 2.00 (m, 1H), 1.66 (m, 3H), 1.50 (m, 1H). C14H16F3N3O=299.12 LCMS (M+H): m/z 300
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08435762B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-2125a0946204422fb05df74e00bee6c7 |
| Source note | uspto-grants-2013_05 |