HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dimethoxybenzoic acid → HCID 45381614, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dimethoxybenzoic acid | HCID 76027 | — |
| Reactant | HCID 45381408 | HCID 45381408 | — |
| Product | HCID 45381614 | HCID 45381614 | — |
Reaction Steps
Title compound was synthesized according to the procedure used in the synthesis of Compound 88S using 2,5-dimethoxybenzoic acid in place of 2,4-dimethoxybenzoic acid. 1H NMR (400 MHz, Acetone-D4) δ (ppm): 7.61 (m, J=4 Hz, 1H), 7.11 (s, 1H), 7.07 (m, J=4 Hz, 1H), 4.07 (m, 1H), 4.00 (s, 3H), 3.80 (s, 3H), 3.34 (s, 3H), 2.89-2.82 (m, 4H), 2.62 (m, 1H), 1.98 (m, 1H), 1.84 (m, 1H), 1.84 (m, 2H), 1.52 (m, 1H). C16H22N2O3=290.16 LCMS (M+H): m/z 291
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08435762B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-c163a065aa9f44c9b5d9ab4a1a4a842d |
| Source note | uspto-grants-2013_05 |