HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxynicotinic acid → HCID 59331197, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxynicotinic acid | HCID 708093 | — |
| Reactant | HCID 44286533 | HCID 44286533 | — |
| Product | HCID 59331197 | HCID 59331197 | — |
Reaction Steps
Title compound was synthesized according to the procedure used in the synthesis of Compound 19S, using 2-methoxynicotinic acid in place of o-methoxybenzoic acid. 1H NMR (400 MHz, CDCl3) δ (ppm): 8.51 (dd, J=8 Hz 1H), 8.28 (dd, J=6 Hz 1H), 7.07 (dd, J=8 Hz 1H), 4.16 (s, 3H, m, 1H), 3.44 (dd, J=12 Hz, 1H), 2.92 (t, J=8 Hz 2H), 2.85 (m, 2H), 2.61 (ddd, J=16, 12 Hz, 1H), 2.03 (m, 1H), 1.75 (m, 3H), 1.59 (m, 1H). C14H19N3O2=261.15 LCMS (M+H): m/z 262
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08435762B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-28b7f54d81024b58b58af68fea6145ef |
| Source note | uspto-grants-2013_05 |