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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2088321Generated: October 31, 2026

2-Methoxynicotinic acid → HCID 59331197, compound

https://huagongshe.com/reaction/2088321

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Methoxynicotinic acidHCID 708093—
ReactantHCID 44286533HCID 44286533—
ProductHCID 59331197HCID 59331197—

Reaction Steps

Title compound was synthesized according to the procedure used in the synthesis of Compound 19S, using 2-methoxynicotinic acid in place of o-methoxybenzoic acid. 1H NMR (400 MHz, CDCl3) δ (ppm): 8.51 (dd, J=8 Hz 1H), 8.28 (dd, J=6 Hz 1H), 7.07 (dd, J=8 Hz 1H), 4.16 (s, 3H, m, 1H), 3.44 (dd, J=12 Hz, 1H), 2.92 (t, J=8 Hz 2H), 2.85 (m, 2H), 2.61 (ddd, J=16, 12 Hz, 1H), 2.03 (m, 1H), 1.75 (m, 3H), 1.59 (m, 1H). C14H19N3O2=261.15 LCMS (M+H): m/z 262

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08435762B2
Source datasetuspto-grants-2013_05
ORD IDord-28b7f54d81024b58b58af68fea6145ef
Source noteuspto-grants-2013_05