HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 86653948, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 58289707 | HCID 58289707 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Product | HCID 86653948 | HCID 86653948 | — |
Reaction Steps
280 mg (0.82 mmol) of tert-butyl {(E)-3-[2-(3-hydroxymethylphenyl)pyrimidin-5-yl]allyl}carbamate are dissolved in 10 ml of THF, shaken at room temperature for 17 h with 300 mg of platinum on active carbon (5%, comprises 56% of water) under a hydrogen atmosphere. The catalyst is filtered off with suction, and the filtrate is evaporated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08435986B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-6c7a93d1229e40ebab3558dfb5a5cfa1 |
| Source note | uspto-grants-2013_05 |