3-Aminopyridine → HCID 58182179, compound

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Reaction Steps

Following the procedures as described in EXAMPLE 1 and starting with 5-(tert-butoxycarbonylamino)-2-phenylthiazole-4-carboxylic acid and 3-aminopyridine, the title compound was obtained as a white solid (21.0 mg, 42%). 1H NMR (400 MHz, DMSO) δ 9.78 (s, 1H), 8.99 (d, J=2.4, 1H), 8.30-8.18 (m, 2H), 7.95-7.88 (m, 2H), 7.59 (s, 2H), 7.53-7.32 (m, 4H). ESIMS m/z=297.1 (M+1).

Provenance & Evidence