HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66955114, compound → HCID 66954979, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66955114 | HCID 66955114 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 66954979 | HCID 66954979 | 83.3% |
Reaction Steps
3-(5-tert-Butoxycarbonylamino-2-fluoro-4-methyl-phenyl)-5-methyl-2H-pyrazole-1-carboxylic acid benzyl ester (320 mg) was hydrogenated using 10% Pd/C (40 mg) following the procedure of step 2 to give 3-(5-amino-2-fluoro-4-methyl-phenyl)-5-methyl-pyrazole-1-carboxylic acid benzyl ester (205 mg) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08435990B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-d514f954469e4879be74ce39000be3eb |
| Source note | uspto-grants-2013_05 |